Jenway 6715 Bedienungsanleitung

67 Series SpectrophotometersOperating Manual670 00

Selecting the copy icon allows the results to be pasted directly into other programmes (e.g. a spreadsheet) for further data manipulation or editing

82File & Data Management Save Tools Print Settings Erase Search Open Save

83If the current user does not have the required privileges to delete the selected method then an information message will be displayed advising that

847.4 PERFORMING MEASUREMENTS – all usersPlace the zero solution in the sample chamber and close the lid.Selecting the Zero key will start the cycle

85SECTION 8 - Kinetics Mode8.1 PRINCIPLES OF MEASUREMENTA number of tests run on a spectrophotometer involve an active ingredient. On addition of

86To enter the required parameters for the sample(s) under test, select the Settings key and the instrument will display the following screen:Mode set

87 Setting WavelengthSelect the Wavelength key and enter the wavelength using the numeric keypad. The Clear key will clear all information

88 Setting Run TimeSelecting the Run Time key displays a numeric keypad. Clear the current setting and enter the required time, in seconds,

89 Setting Start LevelSelecting the Start Level key displays a numeric keypad. Clear the current setting and enter the required level above

90 FactorThis is the value by which the rate of change is multiplied to give the concentration. Select the Factor key and enter the factor

91 Setting Auto-ScaleThe Auto-Scale key toggles between On and Off. With the Auto-Scale function On the instrument will automatically set t

Holding the cursor over the spectrum trace or the data name will highlight the chosen spectrum and fade any other spectra. To return to the origina

92 Setting Batch IDSelect the Batch ID key and enter the batch code using the alphanumeric keypad. Select Enter to accept or Cancel to rema

93 Auto Log Settings…Selecting Auto Log Settings… opens a dedicated sub-menu. This option can be toggled between Off, On and Timed. When th

948.3 LOGGED IN MEASUREMENTPIN Codes – each user is allocated a 4 digit PIN code that is required when logging in. Select Log In… from the Main Me

95 Creating a New MethodTo enter the Method ID, appropriate measurement parameters and the level of Method Security required for the method

96 Selecting Measurement ModeThe Measurement Mode key toggles between Absorbance and Transmittance. Run Settings…Selecting Run S

97 Setting Lag TimeSelecting the Lag Time key displays a numeric keypad. Clear the current setting and enter the required lag time in secon

98 Setting Method SecurityThe 67 Series spectrophotometers can support up to 10 individual users plus one Supervisor who has full administr

99 FactorThis is the value by which the rate of change is multiplied to give the concentration. Select the Factor key and enter the factor

100 Setting Auto-ScaleThe Auto-Scale key toggles between On and Off. With the Auto-Scale function On the instrument will automatically set

101 Setting Batch IDSelect the Batch ID key and enter the batch code using the alphanumeric keypad. Select Enter to accept or Cancel to rem

Selecting the print icon opens the Print box. This allows the user to choose the printer, the orientation of the printout, what data

102 Auto Log Settings…Selecting Auto Log Settings… opens a dedicated sub-menu. This option can be toggled between Off, On and Timed. When t

103File & Data Management Save Tools Print Settings Erase Search Open Save

104Deleting MethodsTo delete methods highlight the required method in the Browse screen as described in Recalling Methods and then touch the Eraser ic

105 8.4 PERFORMING MEASUREMENTS – All UsersWith a method created, or recalled and opened, the kinetics measurement screen is displayed.Before start

106SECTION 9 - Quantitation Mode9.1 PRINCIPLES OF MEASUREMENTThe concentration of a substance in a sample can be found by comparing it to prepared

107To enter the required parameters for the sample(s) under test, select the Settings key and the instrument will display the following screen:Mode se

108 Selecting Measurement ModeThe Measurement Mode key toggles between Absorbance and Transmittance. Setting WavelengthSelect th

109 Selecting UnitsSelection of units is made using the Units key to scroll through the available measurement options. The following units

110 Selecting Calibration StandardsUp to 20 calibration standards may be used to plot the calibration curve (with up to 5 replicates for ea

111 Setting Auto-ScaleThe Auto-Scale key toggles between On and Off. With the Auto-Scale function On the instrument will automatically set

After inputting the required parameters select the tick icon to save the changes or the cross icon to cancel The Results tab displays the data of

112 Selecting Axis ColourSelecting the Axis Colour key displays a colour selection screen. Touch any one of the eight colours to select the

113 Selecting Printer MediaThe Printer Media options toggle between Internal and External Printers. Auto Log Settings…Selecting

1149.3 LOGGED IN MEASUREMENTPIN Codes – Each user is allocated a 4 digit PIN code that is required when logging in.Select Log In… from the Main Menu

115 Creating a New MethodTo enter the Method ID, appropriate measurement parameters and the level of Method Security required for the metho

116 Setting WavelengthSelect the Wavelength key and enter the wavelength using the numeric keypad. The Clear key will clear all information

117 Replicates Setup…Selecting Replicates Setup… opens a dedicated sub-menu.Up to 5 replicates may be selected with the recorded result bei

118 Selecting Calibration StandardsUp to 20 calibration standards may be used to plot the calibration curve (with up to 5 replicates for ea

119 Setting Auto-ScaleThe Auto-Scale key toggles between On and Off. With the Auto-Scale function On the instrument will automatically set

120 Selecting Axis ColourPressing the Axis Colour key displays a colour selection screen. Touch any one of the eight colours to select the

121 Selecting Printer MediaThe Printer Media options toggle between Internal and External Printers. Auto Log Settings…Selecting

The Results tab displays the chosen result. Selecting the rate of change icon displays the following screen. Entering the required Star

122File & Data Management Save Tools Print Settings Erase Search Open Save

123Deleting MethodsTo delete methods highlight the required method in the Browse screen as described in Recalling Methods and then touch the Eraser ic

1249.4 PERFORMING MEASUREMENTS – all usersA minimum of a zero Absorbance calibration must be made before any measurements can be carried out. Havin

125Post Quantitation ToolsAfter construction or recall of a calibration curve the Quantitation Tools can be enabled by pressing the Tools icon on the

126SECTION 10 - Fitting Alternative Modules/Accessories10.1 INTEGRAL PRINTER UNITDisconnect the instrument from the mains supply.The printer lid i

10.2 CELL HOLDER MODULESA number of cell holder module options are available for use with these instruments:• 10x10mm cell holder • 8 cell turret• W

12810.3 AUTOMATIC 8 & 6 CELL CHANGER MODULESOverviewThe automatic 8-cell changer accepts 8 x 10mm path length cuvettes and the automatic 6-cell

129Unpack the new module and check to ensure no damage has occurred during transit. To install the new module raise the lid by 30° and gently ease it

130Installation – 6 Cell Changer CarouselIf your instrument was ordered with the automatic 6 cell changer it will be supplied with the module installe

131If the module has been successfully installed the instrument will show ‘Passed’ alongside the Accessory test… indicator.If the module is incorrectl

Selecting the copy icon allows the results to be pasted directly into other programmes (e.g. a spreadsheet) for further data manipulation or editing

132Cell ConfigurationThe carousel positions are numbered from 0 to 7/5 for the two versions. Selecting the Cell Configu-ration key displays the graphic

13310.4 SIPPER PUMP MODULEOverviewThe Sipper Pump accessory is based on a programmable peristaltic pump that can be set to repeatedly deliver accura

134This is supplied as a complete plug-in module as detailed above. If you are changing from an existing sample chamber module to the sipper pump the

135For traditional sipping:Note: It is recommended that all tubing runs are kept as short as possible. Tubes must not be allowed to obstruct the light

136For pumping:Note: It is recommended that all tubing runs are kept as short as possible. Tubes must not be allowed to obstruct the light path.1. Cut

137Checking the Sipper PumpAfter fitting the tubing it is recommended that the following check is performed to ensure the cuvette fills correctly and th

138Setting Up the Sipper PumpThere are three modes of operation:1. Independent 2. Segmented 3. Bi-Directional1. IndependentThis is similar to

139Calibrating the Sipper PumpFrom the Accessory Settings menu press Calibrate. The following screen is displayed:Offer a sample to the inlet tube in

14010.5 PELTIER MODULEThis accessory module is fitted into the instrument casing by following the instructions for the Cell Accessories. Overview of

141Raise the lid and loosen the sample chamber retaining screw located at the front of the module. Lifting the front carefully remove the module from

Signing Out & Logging In As A Different User Once all of the required data processing has been completed select the sign out icon to return to th

142Setting TemperatureTo set the required temperature select the Set Temperature key and enter the value using the numeric keypad. The Clear key will

14310.6 SIPPER/PELTIER MODULEOverviewThe Sipper Pump accessory is based on a programmable peristaltic pump that can be set to repeatedly deliver acc

144Fitting the Sipper/Peltier Module (as a separate accessory option)This is supplied as a complete plug-in module as detailed above. If you are chang

145The instrument will then perform the power on self-test protocol. The power on and self-test screen will be shown:If the module has been successful

146Sipper Tube Schematic Traditional ‘sipping’ arrangement For pumping:Note: It is recommended that all tubing runs are kept as short as possible. Tub

147Pump Tube SchematicTraditional Pumping Arrangement Checking the Sipper PumpAfter fitting the tubing it is recommended that the following check is pe

148Good Practice GuidelinesSample Size - the cuvette must be filled with solution. If sample volume is limited, the two-stage uptake cycle can be used,

149For draining a flow through cuvette:Note: Whilst using a 1.8 ml flow cell, order numbers 035 025 (glass) and 035 044 (quartz), the sample can only be

150If air segmentation is required remove the sample and press the Start button. View the air being taken up through the polythene tube to the cuvette

151Setting TemperatureTo select the required temperature press the Set Temperature key and enter the value using the numeric keypad. The Clear key wil

67 Series SpectrophotometersModels 6700, 6705 & 6715Operating Manual670 005/REV D/11-11

152SECTION 11 - Maintenance & Troubleshooting11.1 GENERALThe 67 Series are designed to give optimum performance with minimum maintenance. It is

153Tungsten Lamp Replacement – Model 6700Warning: Disconnect the instrument from the mains supply prior to replacing the lamp. Care should be taken wh

154 Flash Lamp Module Replacement – Models 6705 and 6715Warning: Disconnect the instrument from the mains supply prior to replacing the lamp. Care sh

155Important: When fitting the replacement lamp it is essential that the glass is not touched. Finger marks will damage the lamp. Should accidental da

156SECTION 12 - Declaration of Conformity

157SECTION 12 - Declaration of Conformity

158SECTION 12 - Declaration of Conformity

159Touch Screen Mode IconsMode settings (all modes)Accessory options (all modes)Internal or external printer selection (Photometrics mode)Batch ID and

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1 Contents PageSafety 7Guarantee 8SECTION 1 - Introduction 1.1 Instrument Description 91.2 Instrument Specifications 10-111.3 Go

2SECTION 5 - Photometrics Mode5.1 Principles of Measurement 345.2 Free Operation 34-37 Setting Method ID 35 Setting Wavelength 36 Setting

3 Setting Graph Data Points 59 Selecting Printer Media 60 Auto Log Settings… 60 File & Data Management 61-626.4 Performing Measurements

4 Setting Run Time 88 Setting Lag Time 88 Setting Start On Level 88 Setting Start Level 89 Setting Method Security 89 Standard 89 Factor

5 Setting Curve Fit 110 Setting Auto Scale 111 Selecting Plot Colour 111 Selecting Axis Colour 112 Setting Batch ID 112 Setting Graph Data

6

7 Safety This is important information; please read carefully before installing or using this instrument.1. The 67 Series Spectrophotometers are desi

8 Guarantee Please read this important guarantee information:Notwithstanding the description and specification(s) of the instruments contained in the

9 SECTION 1 - Introduction 1.1 INSTRUMENT DESCRIPTIONThe 67 Series offer a range of unique features and functions to help in the management of

101.2 INSTRUMENT SPECIFICATIONSTechnical Specification 6700 6705 6715Light Source Tungsten Halogen Xenon Xenon Spectral Bandwidth 4nm 4nm 1.

11Environmental Operating Conditions:The 67 Series is designed to work safely under the following conditions: Temperature 15 to 40ºCHumidity 0 to 90

IMPORTANT Please ensure the SD Card is fitted into the socket as detailed in the image below. -------------------------------------------

12g) All sample containers must be handled with care; by the top and non-optical surfaces only. Any finger marks evident must be removed using a suitab

13 SECTION 2 - Getting Started2.1 UNPACKING INSTRUCTIONS • Refer to label 1 on carton exterior and ensure instrument type and options/accessories

14If you wish to dispose of the instrument packaging, please do so in an environmentally responsible manner. Please refer to the following guidelines:

152.2.4 TOUCH SCREEN FUNCTIONS1. Standby – this key can be used to enter the standby mode during operation. 2. Instrument Settings – this key can be

162.2.5 TOOLBAR ICONSThe spectrophotometer can be used for making measurements at any time without the need for logging in; but many benefits will b

17Photometrics ModeMode settings – method name, wavelength, method security (if logged in)Accessory options – varies with type of accessory module fitt

18Multi-Wavelength ModeMode settings – method name, measurement type, reading type, sample style, method security (if logged in)Setting wavelengths –

19Kinetics ModeMode settings - method name, wavelength, measurement mode, run settings, method security (if logged in)Calibration – allows setting of

20Quantitation ModeMode settings – method name, measurement mode, wavelength, resolution, units of measurement, replicates set up, method security (if

212.2.6 REAR PANEL LAYOUTPower Switch On/Off switch for the unit.Power In Socket IEC type connection socket for the mains supply cable.Printer Soc

222.2.7 POWER ON AND SELF-TESTSNote: For the Model 6700 allow 30 minutes warm up prior to use.For all models the LCD display may take up to 10 minute

23SECTION 3 - Systems of Operation3.1 MULTI-USER AND FREE OPERATION The 67 Series spectrophotometers focus on secure, multi-user operation. But to

243.2.2 MEMORY HIERARCHYThe top level of the memory hierarchy is the user, defined by a user name and recognised by their unique PIN code. In general

25When successfully logged in the user is returned to the main menu screen from which the required mode of measurement can be selected.The Browse scre

26Deleting MethodsTo delete methods highlight the required method in the Browse screen as described in Recalling Methods and then touch the Erase icon

27SECTION 4 - Instrument Settings4.1 MENU OPTIONS A number of settings can be stored for each signed in user including language, method view setti

284.3.1 ADJUST USER PIN – available to logged in users onlyTo alter your User PIN select the Adjust User PIN key. A warning message will be shown p

294.3.4 TOUCH SCREEN CLICKThe touch screen can be operated with or without an audible click each time a key is touched. The click can be toggled on

304.4 ABOUT Selecting the About key provides information relating to instrument ID and signed in user details. Selecting the OK key returns the inst

314.6.1 INSTRUMENT IDSelecting the Instrument Id: 67XXCVS key allows the supervisor to alter the instrument identification code. This is entered by u

67 Series Spectrophotometer PC Software Installation Insert the 67-Series Software Suite installation CD and select the 67-Series Software Suite

324.6.3.1 CREATE NEW USERSelecting the Create New User key allows the supervisor to enter an additional user on to the instrument using the alphanum

334.6.3.4 RESET USER PINThis option allows the supervisor to reset an individual users PIN code. Select the Reset User PIN option from the screen. T

34SECTION 5 - Photometrics Mode5.1 PRINCIPLES OF MEASUREMENTThe simplest mode of the spectrophotometer is Photometrics. A measurement is made of e

35To enter the appropriate parameters for the sample(s) to be tested select the Settings key and the instrument will display the following screen: Mod

36 Setting WavelengthSelect the Wavelength key and enter the wavelength using the numeric keypad. The Clear key will clear all information

37 Auto Log Settings…Selecting Auto Log Settings… opens a dedicated sub-menu.This option can be toggled between On, Off or Timed.Auto Log S

385.3 LOGGED IN MEASUREMENTPIN Codes – each user is allocated a 4 digit PIN code that is required when logging in. Select Log In… from the Main Men

39 Creating a New MethodSettingsTo enter the Method ID, appropriate wavelength for the sample(s) to be tested and the level of Method Secur

40 Setting Method SecurityThe 67 Series spectrophotometers can support up to 10 individual users plus one Supervisor who has full administr

41 Auto Log Settings…Selecting Auto Log Settings… opens a dedicated sub-menu.This option can be toggled between On, Off or Timed.Auto Log S

When the installation is complete select Close. The 67-Series Software Suite icon is displayed on desktop Getting Started Ensure the P

42File & Data Management Save Tools Print Settings Erase Search Open Save

43Privileges required for deleting designated methods:Public Methods – only the Supervisor and Originator can delete these.Read-Only Methods – only th

5.4 PERFORMING MEASUREMENTS – all usersOnce the required settings have been confirmed the main Photometrics measurement screen will be shown. This sc

45Section 6 - Spectrum Mode6.1 PRINCIPLES OF MEASUREMENTBy examining the absorbance or transmittance of the sample over a wavelength range we can

46Mode settings – method name, measurement mode, wavelength range, plot interval, method security (if logged in)Analysis Points – up to 30 wavelengths

47 Setting WavelengthsNote: If the start or end wavelength is adjusted so that they are closer than twice the plot interval then the previo

48 Selecting Plot IntervalSelecting the Plot Interval key allows the user to toggle between 1.0nm, 5.0nm, 0.1nm and 0.5nm.Using the Back ke

49 Setting Method SecurityThis option is only applicable to logged in users.Setting Additional Set-up Parameters using the Toolbar Icons

50 Setting Auto-ScaleThe Auto-Scale key toggles between On and Off. With the Auto-Scale function On the instrument will automatically set t

51 Selecting Axis ColourSelecting the Axis Colour key displays a colour selection screen. Touch any one of the eight colours to select the

Note: If the selected location does not contain a valid SD card the error message This location does not contain a valid SD card will

52 Selecting Printer MediaThe Printer Media options toggle between Internal and External Printers. Auto Log Settings…Selecting A

536.3 LOGGED IN MEASUREMENTPIN Codes – each user is allocated a 4 digit PIN code that is required when logging in. Select Log In… from the Main Me

54 Creating a New MethodTo enter the Method ID, appropriate measurement parameters and the level of Method Security required for the method

55Setting WavelengthsNote: If the start or end wavelength is adjusted so that they are closer than twice the plot interval then the previously set wav

56 Selecting Plot IntervalSelecting the Plot Interval key allows the user to toggle between 1.0nm, 5.0nm, 0.1nm and 0.5nm.Using the Back ke

57Setting Additional Set-up Parameters using the Toolbar Icons Setting Analysis PointsUp to 30 analysis points can be set be selecting the

58 Setting Auto-ScaleThe Auto-Scale key toggles between On and Off. With the Auto-Scale function On the instrument will automatically set t

59 Selecting Axis ColourSelecting the Axis Colour key displays a colour selection screen. Touch any one of the eight colours to select the

60 Selecting Printer MediaThe Printer Media options toggle between Internal and External Printers. Auto Log Settings…Selecting Auto

61File & Data Management Save Tools Print Settings Erase Search Open Save

required are the same as when logging into the instrument), the user or password can be saved by ticking the appropriate boxes. To access the required

62If the current user does not have the required privileges to delete the selected method then an information message will be displayed advising that

636.4 PERFORMING MEASUREMENTS – all usersPerforming a ScanOnce the required settings have been confirmed the main Spectrum measurement screen will be

64Additional individual samples can be measured by inserting them in the single sample holder and touching Scan. Alternatively, multiple samples can b

65Accepts and re-scales the selected area to the current zoom setting. Selecting the Back key or the Exit Door once maintains the zoom display and giv

66Co-ordinate TaggingToolbar IconsCo-ordinate Tagging Tag Delete TagPeaks, valleys or any other points of interest can be selected (on

67Selecting the Find Peaks & Valleys Table icon displays the peaks and valleys in a table.Scrolling through the table can be carried out using the

68Overlaying ScansToolbar IconSpectral Overlay Add Scans Information Display Display

69Adding or Subtracting SpectraToolbar IconAdd/Subtract Display Display Add Delete

70SECTION 7 - Multi-Wavelength Mode7.1 PRINCIPLES OF MEASUREMENTThe multi-wavelength mode is used to measure absorbance or transmittance at up to

71To enter the required parameters for the sample(s) under test, select the Settings key and the instrument will display the following screen:Mode set

The Results tab displays a table of the all the results in the chosen method. Selecting Filter displays a drop down allowi

72 Selecting Measurement ModeThe Measurement Mode key toggles between Absorbance and Transmittance. Selecting Sample StyleThis o

73 Setting WavelengthsUp to four wavelengths can be set for each measurement parameter. The number of wavelengths to be measured can be set

74(K1A1 + K2A2 + K3A3 + K4A4) x K5K5 x (K1A1 + K2A2) / (K3A3 + K4A4)Primary Wavelength allows the user to select which of the (up to) four wavelengths

75 Auto Log Setting…Selecting the Auto Log Settings… opens a dedicated sub-menu. This option can be toggled between Off, On and Timed. When

767.3 LOGGED IN MEASUREMENTPIN Codes – each user is allocated a 4 digit PIN code that is required when logging in. Select Log In… from the Main Menu

77 Creating a New MethodSettingsTo enter the Method ID, appropriate wavelength for the sample(s) to be tested and the level of Method Secur

78 Selecting Sample StyleThis option allows the user to select to measure one sample at up to four wavelengths, or to measure up to four sa

79 Setting WavelengthsUp to four wavelengths can be set for each measurement parameter. The number of wavelengths to be measured can be set

80(K1A1 + K2A2 + K3A3 + K4A4) x K5K5 x (K1A1 + K2A2) / (K3A3 + K4A4)Primary Wavelength allows the user to select which of the (up to) four wavelengths

81 Auto Log Settings…Selecting the Auto Log Settings… opens a dedicated sub-menu.This option can be toggled between Off, On and Timed . Whe